Development and Characterization of Biodiesel: Analyzing Properties Through GC-MS and Fuel Analyzer
DOI:
https://doi.org/10.38032/scse.2025.3.92Keywords:
Biodiesel, Transesterification, GC-MS, Alternative energy, Fuel analyzerAbstract
This study examines the production and characterization of biodiesel which is derived from soybean oil through the use of a transesterification process. Biodiesel formed via the chemical reaction of soybean oil and methanol in the presence of sodium hydroxide (NaOH) as a catalyst. The resulting biodiesel samples were analyzed using Gas Chromatography-Mass Spectrometry (GC-MS) and Fuel analyzer. The highest yield of methyl ester was obtained by using 60 mL methanol, 250 mL Soyabean oil and 1.4 g NaOH was used as a catalyst. The reaction was carried out at 60 °C for 3h. Among the four primary methyl esters, hexadecenoic acid methyl ester is the dominating ingredient in the combination, with the greatest yield of 11%. The fuel properties of the synthesized biodiesel were evaluated and contrasted with conventional diesel. Notably, the biodiesel exhibited a cetane number of 68.4, considerably higher than that of pure diesel, indicating superior ignition quality. But compared to diesel, biodiesel was shown to have much lower flash and fire points, which could make handling and storage more difficult. These findings show the possibility of soybean oil-derived biodiesel as a viable alternative to traditional diesel, with its higher cetane number enabling increased combustion efficiency. Nevertheless, the decreased flash and fire thresholds demand more work to improve the safety properties of the biodiesel.
Downloads
Downloads
Downloads
References
1. Saifullah, A., A. Karim, and M.R. Karim, Advancement of biodiesel in Bangladesh. IOSR Journal of Engineering (IOSRJEN), 2016. 6: p. 59-64.
2. You, Y.-D., et al., Economic cost analysis of biodiesel production: case in soybean oil. Energy & Fuels, 2008. 22(1): p. 182-189.
3. Hoekman, S.K., et al., Review of biodiesel composition, properties, and specifications. Renewable and sustainable energy reviews, 2012. 16(1): p. 143-169.
4. Kulkarni, M.G. and A.K. Dalai, Waste cooking oil an economical source for biodiesel: a review. Industrial & engineering chemistry research, 2006. 45(9): p. 2901-2913.
5. Usman, A., et al., Fatty acid methyl esters composition of Trichilia emetica shell oil. Am Sci Res J Eng Technol Sci, 2016. 21(1): p. 83-90.
6. Noureddini, H. and D. Zhu, Kinetics of transesterification of soybean oil. Journal of the American Oil Chemists' Society, 1997. 74: p. 1457-1463.
7. Demirbas, A. and A. Biodiesel, A realistic fuel alternative for diesel engines. London: Springer-Verlag. ISBN, 2008. 10: p. 1846289947.
8. Kulišić, B., et al., Impacts of biodiesel production on Croatian economy. Energy Policy, 2007. 35(12): p. 6036-6045.
9. Lee, D.-H., Algal biodiesel economy and competition among bio-fuels. Bioresource technology, 2011. 102(1): p. 43-49.
10. Mukhopadhyay, K., X. Chen, and P. Thomassin, Economy wide impacts of ethanol and biodiesel policy in Canada: An input–output analysis. International Journal of Green Energy, 2017. 14(4): p. 400-415.
11. Naylor, R.L. and M.M. Higgins, The political economy of biodiesel in an era of low oil prices. Renewable and Sustainable Energy Reviews, 2017. 77: p. 695-705.
12. Xing, A., et al., Life cycle assessment of economy for biodiesel. Journal of Tsinghua University Science and Technology, 2010. 50(6): p. 923-927.
13. Borugadda, V.B. and V.V. Goud, Biodiesel production from renewable feedstocks: Status and opportunities. Renewable and Sustainable Energy Reviews, 2012. 16(7): p. 4763-4784.
14. Mahlia, T., et al., Patent landscape review on biodiesel production: Technology updates. Renewable and Sustainable Energy Reviews, 2020. 118: p. 109526.
15. Hassan, M.H. and M.A. Kalam, An overview of biofuel as a renewable energy source: development and challenges. Procedia engineering, 2013. 56: p. 39-53.
16. Kumar, P., M.P. Sharma, and G. Dwivedi, Impact of ternary blends of biodiesel on diesel engine performance. Egyptian Journal of Petroleum, 2016. 25(2): p. 255-261.
17. Dhar, A. and A.K. Agarwal, Effect of Karanja biodiesel blend on engine wear in a diesel engine. Fuel, 2014. 134: p. 81-89.
18. Habibullah, M., et al., Potential of biodiesel as a renewable energy source in Bangladesh. Renewable and Sustainable Energy Reviews, 2015. 50: p. 819-834.
19. Statista. Production of natural gas worldwide in 2023, by country. 2024; Available from: https://www.statista.com/statistics/264101/world-natural-gas-production-by-country/.
20. Gas reserve to last until 2031. 2015; Available from: https://www.thedailystar.net/news/bangladesh/news/benazirs-immovable-properties-court-appoints-administrators-look-after-them-3628866.
21. Rahman, M.S., et al., Present situation of renewable energy in Bangladesh: renewable energy resources existing in Bangladesh. Global Journal of Researches in Engineering Electrical and Electronics Engineering, 2013. 13(5): p. 1.
22. Reza, S.E., T.A. Nitol, and I. Abd-Al-Fattah, Present scenario of renewable energy in Bangladesh and a proposed hybrid system to minimize power crisis in remote areas. International journal of renewable energy research, 2012. 2(2): p. 280-288.
23. Anam, K. and H. Bustam, Power crisis & its solution through renewable energy in Bangladesh. Cyber Journals: Multidisciplinary Journals in Science and Technology, Journal of Selected Areas in Renewable and Sustainable Energy (JRSE), 2011: p. 13-18.
24. Lin, L., et al., Biodiesel production from crude rice bran oil and properties as fuel. Applied energy, 2009. 86(5): p. 681-688.
25. Poth, U., Drying oils and related products. Ullmann's Encyclopedia of Industrial Chemistry, 2000.
Published
Conference Proceedings Volume
Section
License
Copyright (c) 2025 Md. Anowar Hossain, Ummey Rayhan, Md. Mamun, Anik Talukder, Fatema Tuz Zahra, Shuvo Chandra Das (Author)

This work is licensed under a Creative Commons Attribution 4.0 International License.
All the articles published by this journal are licensed under a Creative Commons Attribution 4.0 International License
